称取一定量的工业钼粉，放入行星式球磨机中，在氩气保护下球磨24 h，每球磨1 h停机8~10 min，同时改变球磨机转动方向，球料比为10：1；球磨转速为100 r/min和200 r/min，所得钼粉标记为Mo-100r和Mo-200r。对球磨后钼粉使用XRD对粉末进行物相分析，步长8°/min，范围10~90°。将球磨后粉末加入含酒精的试管中超声震荡15min分散后，通过扫描电镜采集粉末形貌图像，并利用所采集的粉末SEM图像统计粉末粒径。

A certain amount of industrial molybdenum powder was weighed, put into a planetary ball mill, and ball milled for 24 h under argon protection, with a stoppage of 8~10 min for every 1 h of ball milling, while changing the rotation direction of the ball mill, with a ball-to-material ratio of 10:1; the ball milling speed was 100 r/min and 200 r/min, and the resulting molybdenum powder was labeled Mo-100r and Mo-200r. The molybdenum powder after ball milling was analyzed by XRD for powder The powder was analyzed by XRD with a step size of 8°/min and a range of 10-90°. The powder was added to a test tube containing alcohol and dispersed by ultrasonic shaking for 15 min, and the powder morphology images were collected by scanning electron microscopy, and the powder SEM images were used to calculate the powder size.